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Containerless Measurements of High Temperature Material Properties

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dc.contributor.advisorRobert W Hyers
dc.contributor.authorCanepari, Stacy M
dc.contributor.departmentUniversity of Massachusetts Amherst
dc.contributor.departmentMechanical Engineering
dc.date2023-09-22T20:04:45.000
dc.date.accessioned2024-04-26T21:04:03Z
dc.date.available2009-06-30T00:00:00Z
dc.date.issued2009-01-01
dc.date.submitted2009-September
dc.description.abstractCurrently, the design of high temperature mechanical components is limited by material performance at elevated temperatures. Rocket nozzle materials, for example, need to survive exhaust gas temperatures up to 3000 ºC under high stresses for short periods of time. Additionally, one of the current challenges in hypersonic flight is the development of materials that will withstand the leading edge temperatures which exceed 2700 ºC. In these severe environments, the characterization of materials’ creep properties is essential. Conventional creep testing methods are limited to 1700°C. Using ESL, a group of researchers at the University of Massachusetts Amherst developed a non-contact creep method, which is not subject to such temperature limits. Using the non-contact method a spherical sample is rotated rapidly, and the driving load is applied by centripetal acceleration, which causes deformation. During previous creep tests, a laser supplied both the heating and driving rotational force to the sample. Since the rotation is controlled by the photon pressure emitted from the heating laser, the applied stress is coupled to the testing temperature. By developing an independent rotation control, non-contact creep tests could be conducted on a wider range of materials. A specialized high-speed induction motor was developed for use in high-temperature creep tests. In addition to creep behavior, the understanding of thermophysical properties is important for the emerging class of high temperature material. Using a previously developed method, non-contact density measurements were taken concurrently on the same materials as X-ray diffraction measurements. Over 35 materials were successfully processed including, aluminum, copper, hafnium, palladium, nickel, titanium and zirconium based alloys. Besides contributing to high temperature material databases, density measurements provide an understanding of solidus formation and short-range order in the liquid state.
dc.description.degreeMaster of Science in Mechanical Engineering (M.S.M.E.)
dc.identifier.doihttps://doi.org/10.7275/884646
dc.identifier.urihttps://hdl.handle.net/20.500.14394/46871
dc.relation.urlhttps://scholarworks.umass.edu/cgi/viewcontent.cgi?article=1403&context=theses&unstamped=1
dc.source.statuspublished
dc.subjectMechanical engineering
dc.subjectcreep
dc.subjecthigh temperature material
dc.titleContainerless Measurements of High Temperature Material Properties
dc.typecampus
dc.typearticle
dc.typethesis
digcom.contributor.authorisAuthorOfPublication|email:stacy.canepari@gmail.com|institution:University of Massachusetts Amherst|Canepari, Stacy M
digcom.date.embargo2009-06-30T00:00:00-07:00
digcom.identifiertheses/321
digcom.identifier.contextkey884646
digcom.identifier.submissionpaththeses/321
dspace.entity.typePublication
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